Nitric Acid, ASTM A, Practice C, (Huey Test) The specimens are boiled for five periods, each of 48 hours, in a 65 per cent solution of nitric acid. The corrosion. employed to measure the relative susceptibility of austenitic stainless steels to intergranular attack. ASTM A Practice C, boiling nitric acid test is also known . Ferric Sulfate – Sulfuric Acid, ASTM A – Practice B (Stretcher Test). Ferric Sulfate Nitric Acid, ASTM A, Practice C, (Huey Test). Nitric Acid, ASTM A

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The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as sigma phase, and is also used for materials in z262 oxidizing environments such as nitric acid.

Classification of the structure after A Practice A analysis will determine if the material is acceptable or if additional testing is required.

Corrosion Testing

It is informational only and not an official part of the standard; the full text of the standard itself must be referred to for its use and application. Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard. View pfactice articles about Aerospace Oil w262 Gas Transportation. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

This test is used exclusively to determine corrosion in areas high in chromium carbide formations, and is not as effective for intergranular attack caused by other means. If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly treated materials; ASTM A is a screening test to help find batches that are incorrectly processed.


Because it can be run quickly for screening, we often run this test first. This simple etching technique is used as a quick screening method to ensure that a material is free of intergranular corrosion susceptibility.

For example, many low-carbon and stabilized stainless steels e. Historical Version s – view previous versions of standard. This abstract is a brief summary of the referenced standard.

Strauss test specimens are boiled in a Copper Sulfate – Sulfuric Acid mixture for 15 hours. Sensitization causes the grain boundaries of a material to precipitate, creating pracice deposits and causing the material to be susceptible to intergranular attack.

Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself. The weight loss is calculated after each step, and reveals if the sample has been properly heat-treated.

It is typically used for stainless alloys such as andCr-Ni-Mo stainless alloys, and nickel alloys to evaluate the intergranular attack associated with the precipitation of chromium carbides at grain boundaries. Practice E, the Strauss test, is adtm to assess attack associated with chromium-rich carbide formation; it does not detect susceptibility to sigma phase formation.

At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established corrosion rate for that specific material type. These practices include five intergranular corrosion tests, namely: The level of corrosion is determined by mass loss.


Testing Services

From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment. The Oxalic Acid test is only used to ensure that no corrosion exists; samples are labeled either “Acceptable” or “Suspect”.

The etch structure types used to classify the specimens are: A recent publication on intergranular corrosion. Work Item s – proposed revisions of this standard.

ASTM A Intergranular Corrosion Testing and Analysis

Based on your materials, application, and requirements, the other 4 methods provide specific focuses. G2MT Labs is one of the few labs to offer all five ASTM A corrosion testing practices, as well as the expertise to help you determine which tests to use, what to do if a test fails, and other corrosion consulting as needed.

Like what you saw? Intergranular lractice shows up as the dark black lines around the grain boundaries. However, when a material is exposed to high temperatures for long periods of time, a process called sensitization may occur.

Intergranular Corrosion Testing: An Overview of ASTM A262

Learn more about our laboratories – where they parctice located; the unique capabilities they have and how they can help you solve your technical and commercial challenges. The Copper Sulfate Test is especially effective for determining susceptibility to intergranular attack for low carbon steels. The first and fastest step is the ASTM A Practice A, a rapid same-day screening method in Oxalic acid to determine the susceptibility to intergranular corrosion.

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